HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl Peroxide → HCID 20092923, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl Peroxide | HCID 7187 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | 4-(4-Methylphenyl)-5-pyrimidinecarbonitrile | HCID 20092943 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 20092923 | HCID 20092923 | 105.5% |
Reaction Steps
A mixture of 5-cyano-4-(p-tolyl)pyrimidine (2.5 g, 12.8 mmol), N-bromosuccinimide (2.4 g, 13.5 mmol) and benzoyl peroxide (catalytic amount) in carbon tetrachloride (100 ml) was refluxed under light radiation for 1 hour. After cooling, insoluble materials were removed and the filtrate was concentrated to dryness to afford a yellow syrup (3.7 g, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05389641 |
| Source dataset | uspto-grants-1995_02 |
| ORD ID | ord-8a0010ea70a54f8cb71f7da42286d8b5 |
| Source note | uspto-grants-1995_02 |