HCID 20093424, compound → HCID 178439990, compound

HRID 274623Notes

Reaction equation

HRID 274623 reaction equation
[CH3:1][N:2]1[C:6]2[N:7]([CH2:13][C:14]3[CH:19]=[CH:18][C:17]([C:20]4[CH:25]=[CH:24][CH:23]=[CH:22][C:21]=4[C:26]4[N:30](C(C5C=CC=CC=5)(C5C=CC=CC=5)C5C=CC=CC=5)[N:29]=[N:28][N:27]=4)=[CH:16][CH:15]=3)[C:8]([CH2:10][CH2:11][CH3:12])=[N:9][C:5]=2[N:4]=[C:3]1[CH3:50]>CC(O)=O>[CH3:1][N:2]1[C:6]2[N:7]([CH2:13][C:14]3[CH:15]=[CH:16][C:17]([C:20]4[CH:25]=[CH:24][CH:23]=[CH:22][C:21]=4[C:26]4[NH:30][N:29]=[N:28][N:27]=4)=[CH:18][CH:19]=3)[C:8]([CH2:10][CH2:11][CH3:12])=[N:9][C:5]=2[N:4]=[C:3]1[CH3:50]

Participants

3

Reactant 1

HCID 20093424HCID 20093424, compound

Product 1

HCID 178439990HCID 178439990, compound

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

1,6-Dihydro-1.2-dimethyl-5-propyl-6-[(2'-{N-triphenylmethyltetrazol-5-yl}{1,1'-biphenyl}-4-yl)-methyl]imidazo[4,5-d]imidazole prepared as described above in Step F can be deblocked with aqueous HOAc at 50° C. as described for a related procedure (see Example 11, Step F) to give the title compound.

Sources & evidence

ORD record
ord-3080a224e5de411a95ba6039dc44f8ad
Source dataset
uspto-grants-1995_02
Patent number
US05389660

Reaction notes

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