HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propionyl chloride → HCID 23343022, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propionyl chloride | HCID 62324 | — |
| Reactant | 2-(4-Carboxybenzamido)-4-aminobenzoic acid | HCID 23343038 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 23343022 | HCID 23343022 | 62% |
Reaction Steps
The procedure of Example 4 was repeated to react 2-(4-carboxybenzamido)-4-aminobenzoic acid with propionyl chloride, and the reaction product was treated as in Example 4 except that isopropyl alcohol was used as a solvent for recrystallization. The product obtained was a 62% yield of 2-(4-carboxybenzamido)-4-propionamidobenzoic acid having a melting point in the range of from 284° to 286° C. (decompose).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04221814 |
| Source dataset | uspto-grants-1980_09 |
| ORD ID | ord-47e35bb137994dbc9816a068225b13f4 |
| Source note | uspto-grants-1980_09 |