HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 274756Generated: October 29, 2026
Sulfur → Ethyl (7-methoxynaphthalen-1-yl)acetate
https://huagongshe.com/reaction/274756
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sulfur | HCID 5362487 | — |
| Reactant | Ethyl (7-methoxy-1,2,3,4-tetrahydro-1-naphthylidene)acetate | HCID 53884445 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | Ethyl (7-methoxynaphthalen-1-yl)acetate | HCID 13570063 | — |
Reaction Steps
50 g of ethyl 7-methoxy-1,2,3,4-tetrahydro-1-naphthylideneacetate are mixed with 7.35 g of sulphur, and the mixture is heated at 215° C. for 10 hours. It is cooled, 300 cm3 of ethyl acetate are added, and the mixture is stirred for 30 minutes and filtered. It is then dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05389683 |
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| Source dataset | uspto-grants-1995_02 |
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| ORD ID | ord-30763dec74354121983a0106daade80d |
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| Source note | uspto-grants-1995_02 |
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