Benzenesulfonyl chloride, 4-chloro-3-nitro- → HCID 178428649, compound
Reaction equation
[NH:1]1[C:5]2[CH:6]=[CH:7][C:8]([CH2:10][CH:11]([NH2:21])[C:12]([N:14]3[CH2:19][CH2:18][CH:17]([CH3:20])[CH2:16][CH2:15]3)=[O:13])=[CH:9][C:4]=2[N:3]=[CH:2]1.[Cl:22][C:23]1[CH:28]=[CH:27][C:26]([S:29](Cl)(=[O:31])=[O:30])=[CH:25][C:24]=1[N+:33]([O-:35])=[O:34]>>[NH:1]1[C:5]2[CH:6]=[CH:7][C:8]([CH2:10][CH:11]([NH:21][S:29]([C:26]3[CH:27]=[CH:28][C:23]([Cl:22])=[C:24]([N+:33]([O-:35])=[O:34])[CH:25]=3)(=[O:30])=[O:31])[C:12]([N:14]3[CH2:19][CH2:18][CH:17]([CH3:20])[CH2:16][CH2:15]3)=[O:13])=[CH:9][C:4]=2[N:3]=[CH:2]1Participants
3
Procedure
Prepared from 1-(1H-benzimidazol-5-yl-methyl)-2-(4-methyl-piperidin-1-yl)-2-oxo-ethylamine and 4-chloro-3-nitro-benzenesulphonic acid chloride analogously to Example 2.
Sources & evidence
- ORD record
- ord-fc50543d15594d678f672712553c5fe7
- Source dataset
- uspto-grants-1995_02
- Patent number
- US05391556
Reaction notes
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