2-Nitrobenzenesulfonyl chloride → HCID 178428647, compound
Reaction equation
[NH:1]1[C:5]2[CH:6]=[CH:7][C:8]([CH2:10][CH:11]([NH2:21])[C:12]([N:14]3[CH2:19][CH2:18][CH:17]([CH3:20])[CH2:16][CH2:15]3)=[O:13])=[CH:9][C:4]=2[N:3]=[CH:2]1.[N+:22]([C:25]1[CH:30]=[CH:29][CH:28]=[CH:27][C:26]=1[S:31](Cl)(=[O:33])=[O:32])([O-:24])=[O:23]>>[NH:1]1[C:5]2[CH:6]=[CH:7][C:8]([CH2:10][CH:11]([NH:21][S:31]([C:26]3[CH:27]=[CH:28][CH:29]=[CH:30][C:25]=3[N+:22]([O-:24])=[O:23])(=[O:32])=[O:33])[C:12]([N:14]3[CH2:19][CH2:18][CH:17]([CH3:20])[CH2:16][CH2:15]3)=[O:13])=[CH:9][C:4]=2[N:3]=[CH:2]1Participants
3
Procedure
Prepared from 1-(1H-benzimidazol-5-yl-methyl)-2-(4-methyl-piperidin-1-yl)-2-oxo-ethylamine and 2-nitrobenzenesulphonic acid chloride analogously to Example 2.
Sources & evidence
- ORD record
- ord-4257d24d6ad247ca851886e54211194b
- Source dataset
- uspto-grants-1995_02
- Patent number
- US05391556
Reaction notes
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