HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → alpha,2,6-Trimethylmorpholin-4-ylethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Triisopropanolamine | HCID 24730 | — |
| Product | alpha,2,6-Trimethylmorpholin-4-ylethanol | HCID 98999 | — |
Reaction Steps
3 g of tris-(2-hydroxypropyl)amine and 1 g of SnO2 doped with sulfuric acid were heated in a manner similar to that described in Example 3 for a period of 1 h at 250° C. There were obtained, in addition to 50 wt % of educt, 30 wt % of N-(2-hydroxypropyl)-2,6-dimethylmorpholine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05391734 |
| Source dataset | uspto-grants-1995_02 |
| ORD ID | ord-b688cab9275c4fb6885fb2fc7cb74e14 |
| Source note | uspto-grants-1995_02 |