HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 275251Generated: October 26, 2026
2-Methylbenzothiazole → 2-Methyl-3-(5-carboxypentyl) benzothiazolium bromide
https://huagongshe.com/reaction/275251
Participants
| Role | Name | HCID | Charge |
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| Reactant | 2-Methylbenzothiazole | HCID 8446 | — |
| Reactant | 6-Bromohexanoic acid | HCID 20210 | — |
| Product | 2-Methyl-3-(5-carboxypentyl) benzothiazolium bromide | HCID 22930888 | 212.9% |
Reaction Steps
2-methyl benzothiazole (19.5g, 0.1M) and 6-bromohexanoic acid (15.3g, 0.1M) were mixed and heated at 120° C. for 4 hours under continuous agitation. The resulting solid was broken up, ground with ether and then filtered. The filtrate was washed with more ether (250ml) to yield an off-white powder (57.5g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05393654 |
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| Source dataset | uspto-grants-1995_02 |
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| ORD ID | ord-e9b9ffc8121942548db3ebc77f1545c8 |
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| Source note | uspto-grants-1995_02 |
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