Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Phenyl-1,3-propanediol → Hydroxypropiophenone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Phenyl-1,3-propanediol | HCID 572059 | — |
| 반응물 | (1S)-1-phenylpropane-1,3-diol | HCID 6950537 | — |
| 용매 | Isopropanol hexane | HCID 21585144 | — |
| 생성물 | Hydroxypropiophenone | HCID 569605 | — |
반응 단계
Determination of the absolute configuration, optical purity and reaction yield of 1-phenyl-1,3-propanediol or a derivative thereof in the examples was determined by high pressure liquid chromatography (column: Chiral Cell OB, manufactured by Daisel Chemical Co., eluent: hexane/2-propanol (8/2), flow rate: 0.7 ml/min, detection: UV 210 nm). The reaction yield represents the mole percentage of (S)-1-phenyl-1,3-propanediol produced per mole of 1-phenylpropan-3-ol-1-one added as starting material.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05393664 |
| 출처 데이터셋 | uspto-grants-1995_02 |
| ORD ID | ord-4ea4684372744d47a2f4a72e51f79258 |
| 출처 메모 | uspto-grants-1995_02 |