Benzenesulfonyl chloride → HCID 19800028, compound

HRID 275301Notes

Reaction equation

HRID 275301 reaction equation
[NH2:1][CH2:2][CH2:3][C:4]([O:6][CH3:7])=[O:5].[C:8]1([S:14](Cl)(=[O:16])=[O:15])[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1>>[C:8]1([S:14]([NH:1][CH2:2][CH2:3][C:4]([O:6][CH3:7])=[O:5])(=[O:16])=[O:15])[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1

Participants

3

Reactant 2

HCID 7369Benzenesulfonyl chlorideHCID 192794Methyl beta-alanate

Product 1

HCID 19800028HCID 19800028, compound

Procedure

N-(phenylsulfonyl)-β-alanine, methyl ester (23) was prepared from methyl β-alaninate and phenylsulfonyl chloride on a 32 mmol scale in the manner described above in Example 13 to yield 6.76 g (86%) of product.

Sources & evidence

ORD record
ord-542fbd231af14a1ba22fab88875ad003
Source dataset
uspto-grants-1995_02
Patent number
US05393747

Reaction notes

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