HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylene Glycol → Methyl 2-methyl-1,3-dioxolane-2-butanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylene Glycol | HCID 174 | — |
| Reactant | Methyl 5-oxohexanoate | HCID 84129 | — |
| Product | Methyl 2-methyl-1,3-dioxolane-2-butanoate | HCID 3310317 | — |
Reaction Steps
Methyl 2-methyl-1,3-dioxolane-2-butanoate (25) was prepared from methyl 5-oxohexanoate and ethylene glycol in the manner described in Example 17 above on a 28 mmol scale to yield 4.94 g (94%) of product. The product was employed immediately in the manner described in Example 26 below.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05393747 |
| Source dataset | uspto-grants-1995_02 |
| ORD ID | ord-ba8293fb5240431eb4f2b315ab18fc2c |
| Source note | uspto-grants-1995_02 |