Phosgene → HCID 20087710, compound

HRID 275314Notes

Reaction equation

HRID 275314 reaction equation
[C:1]([Cl:4])(Cl)=[O:2].[Cl:5][C:6]1[CH:7]=[CH:8][C:9]2[O:15][C:14]3[CH:16]=[CH:17][CH:18]=[CH:19][C:13]=3[NH:12][CH2:11][C:10]=2[CH:20]=1>>[Cl:5][C:6]1[CH:7]=[CH:8][C:9]2[O:15][C:14]3[CH:16]=[CH:17][CH:18]=[CH:19][C:13]=3[N:12]([C:1]([Cl:4])=[O:2])[CH2:11][C:10]=2[CH:20]=1

Participants

3

Reactant 2

HCID 6371PhosgeneHCID 15410465HCID 15410465, compound

Product 1

HCID 20087710HCID 20087710, compound

Procedure

2-chlorodibenz[b,f][1,4]oxazepine-10(11H)-carbonyl chloride (43) is prepared in the manner described in Example 2 using phosgene and 2-chloro-10,11-dihydrodibenz[b,f][1,4]-oxazepine (42), prepared in the manner described above in Example 42.

Workup

  1. customprepared in the manner

Sources & evidence

ORD record
ord-625c962db92c4e49bd536d22fba8f875
Source dataset
uspto-grants-1995_02
Patent number
US05393747

Reaction notes

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