Ethylene Glycol → HCID 13781049, compound

HRID 275381Notes

Reaction equation

HRID 275381 reaction equation
[C:1]([C:4]1[CH:11]=[CH:10][C:7]([CH2:8]Cl)=[C:6]([CH2:12][CH2:13][CH3:14])[C:5]=1[OH:15])(=[O:3])[CH3:2].[CH2:16]([OH:19])[CH2:17][OH:18]>>[C:1]([C:4]1[CH:11]=[CH:10][C:7]([CH2:8][O:18][CH2:17][CH2:16][OH:19])=[C:6]([CH2:12][CH2:13][CH3:14])[C:5]=1[OH:15])(=[O:3])[CH3:2]

Participants

3

Reactant 2

HCID 174Ethylene GlycolHCID 137810224-Acetyl-3-hydroxy-2-propylbenzyl chloride

Product 1

HCID 13781049HCID 13781049, compound

Procedure

Following the procedure of Example 48, 6.8 g. of 4-acetyl-3-hydroxy-2-propylbenzyl chloride and 150 ml. of ethylene glycol were reacted to provide 4.6 g. of the title alcohol. NMR.

Workup

  1. customto provide 4.6 g

Sources & evidence

ORD record
ord-a084e3366aa04d729b125fe019d92d42
Source dataset
uspto-grants-1995_02
Patent number
US05393768

Reaction notes

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