HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Ethyl-3-(3'-dimethylaminopropyl)carbodiimide → HCID 20088290, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Ethyl-3-(3'-dimethylaminopropyl)carbodiimide | HCID 15908 | — |
| Reactant | 2-Dimethylaminopyridine | HCID 21885 | — |
| Reactant | 4-Pyridinemethanamine | HCID 77317 | — |
| Reactant | HCID 15232861 | HCID 15232861 | — |
| Product | HCID 20088290 | HCID 20088290 | — |
Reaction Steps
Using a solution of N-[2-(3-cyclopentyloxy-4-methoxyphenyl)ethyl]oxamic acid (284 mg, 0.92 mmol), EDAC (220 mg, 1.16 mmol) and dimethylaminopyridine (140, 1.25 mmol) and 4-aminomethyl pyridine in an analogous method to that of Example 12 above provided the title compound yielding (126 mg, 34%): m.p. 129°-131° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05393788 |
| Source dataset | uspto-grants-1995_02 |
| ORD ID | ord-68fb1b88680a47cb909c663533a9e1f1 |
| Source note | uspto-grants-1995_02 |