Bromotrimethylsilane → HCID 20088782, compound

Participants

Reaction Steps

To a solution of 31.2 g (0.1 mole) of 3,5-bis-(1,1-dimethylethyl)-4-hydroxy-α-phenylbenzenemethanol (Example 16) in 350 mL of CCl4 is added 34.8 (0.227 mole) of bromotrimethylsilane. After 40 minutes at room temperature the reaction mixture is evaporated to dryness on a rotary evaporator with the water bath temperature at 35° C. The brown oil residue is used immediately without further purification.

Provenance & Evidence