HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromine → 1-Acetyl-5-bromo-2,3-dihydro-3-[2-(methanesulphonyl)ethyl]-1h-indole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | 1-Acetyl-2,3-dihydro-3-[2-(methanesulphonyl)ethyl]-1H-indole | HCID 18545886 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 1-Acetyl-5-bromo-2,3-dihydro-3-[2-(methanesulphonyl)ethyl]-1h-indole | HCID 18545809 | — |
Reaction Steps
Bromination was done by treatment of 19a with bromine in a mixture of acetic acid and dichloromethane. The compound was an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06352988B2 |
| Source dataset | uspto-grants-2002_03 |
| ORD ID | ord-93d00a0346234615bb5b0263e1772823 |
| Source note | uspto-grants-2002_03 |