HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 275769Generated: October 26, 2026
Dimethylformamide dimethyl acetal → HCID 57012287, compound
https://huagongshe.com/reaction/275769
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | Methyl 4-pyridylacetate | HCID 122482 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 57012287 | HCID 57012287 | — |
Reaction Steps
Methyl-4-pyridinylacetate (6.3 g) was dissolved in N,N-dimethylformamide (30 cm3) treated with N,N-dimethylformamide dimethyl acetal (15 cm3) and heated at 80° C. for 2 h. The reaction was then cooled and evaporated under high vacuum to afford crude methyl-3-dimethylamino-2-(pyridin-4-yl)propenoate (7.3 g) which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06352994B2 |
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| Source dataset | uspto-grants-2002_03 |
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| ORD ID | ord-ba11308f8f6045e8abcfcf0a875f5080 |
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| Source note | uspto-grants-2002_03 |
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