HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Benzylphenylacetamide → 3-Benzyl-1-cyanomethylbenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Benzylphenylacetamide | HCID 18317005 | — |
| Reactant | 3-Benzylphenylacetamide | HCID 18317008 | — |
| Product | 3-Benzyl-1-cyanomethylbenzene | HCID 18317010 | — |
Reaction Steps
The two cyanomethyl intermediates, prepared above, were converted via the H202 conditions of Example 2 to their corresponding crystalline amides: 4-benzylphenylacetamide (93%), melting at 183-84° C. and 3-benzylphenylacetamide (59%), melting at 136-37° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06353128B1 |
| Source dataset | uspto-grants-2002_03 |
| ORD ID | ord-8c7af49f7cd6464dae35d0276a912c4c |
| Source note | uspto-grants-2002_03 |