Thionyl Chloride → HCID 18316300, compound

HRID 276315Notes

Reaction equation

HRID 276315 reaction equation
O[CH2:2][CH2:3][NH:4][CH2:5][CH:6]([CH3:9])[CH2:7][CH3:8].O=S(Cl)[Cl:12]>>[Cl-:12].[Cl:12][CH2:2][CH2:3][NH2+:4][CH2:5][CH:6]([CH3:9])[CH2:7][CH3:8]

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 2963742-(2-METHYLBUTYLAMINO)ETHANOL

Product 1

HCID 18316300HCID 18316300, compound

Procedure

N-(2-Hydroxyethyl)-N-(2-methylbutyl)amine was reacted with SOCl2 according to Method B7a to give N-(2-chloroethyl)-N-(2-methylbutyl)ammonium chloride. The chloroethylamine was reacted with 2-methyl-4-nitrophenyl isothiocyanate according to Method C1a to give to give 2-(2-methyl-4-nitrophenylimino)-3-(2-methyl-1-butyl)-1,3-thiazolidine.

Sources & evidence

ORD record
ord-dc1375d366df4b4a84c370bb2524ade5
Source dataset
uspto-grants-2002_03
Patent number
US06353006B1

Reaction notes

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