HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanolamine → N-cycloheptylmethyl-N-(2-hydroxyethyl)amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanolamine | HCID 700 | — |
| Reactant | (Bromomethyl)cycloheptane | HCID 23000753 | — |
| Product | N-cycloheptylmethyl-N-(2-hydroxyethyl)amine | HCID 18316190 | — |
Reaction Steps
2-Hydroxyethylamine was reacted with cycloheptylmethyl bromide according to Method B2a to give N-cycloheptylmethyl-N-(2-hydroxyethyl)amine. The alcohol was reacted with SOCl2 according to Method B7c to give N-cycloheptylmethyl -N-(2-chloroethyl)ammonium chloride. The chloroethylamine was reacted with 2,3-dichlorophenyl isothiocyanate to give 2-(2,3-dichlorophenylimino)-3-(cycloheptylmethyl)-1,3-thiazolidine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06353006B1 |
| Source dataset | uspto-grants-2002_03 |
| ORD ID | ord-f0a9edcf5d744533bd707236b6fcb5b0 |
| Source note | uspto-grants-2002_03 |