3-Bromo-2-methyl-1-propene → HCID 86590181, compound

HRID 276525Notes

Reaction equation

HRID 276525 reaction equation
[CH3:1][C:2]1[CH:7]=[C:6]([N+:8]([O-:10])=[O:9])[CH:5]=[CH:4][C:3]=1[N:11]=[C:12]1[NH:16][CH2:15][C:14]([CH3:18])([CH3:17])[S:13]1.[CH3:19][C:20](=[CH2:23])[CH2:21][Br:22]>>[BrH:22].[CH3:1][C:2]1[CH:7]=[C:6]([N+:8]([O-:10])=[O:9])[CH:5]=[CH:4][C:3]=1[N:11]=[C:12]1[N:16]([CH2:21][C:20]([CH3:23])=[CH2:19])[CH2:15][C:14]([CH3:18])([CH3:17])[S:13]1

Participants

3

Reactant 2

HCID 3577853-Bromo-2-methyl-1-propeneHCID 178428744HCID 178428744, compound

Product 1

HCID 86590181HCID 86590181, compound

Procedure

2-Methyl-2-hydroxypropylamine was reacted with SOCl2 followed by 2-methyl-4-nitrophenyl isothiocyanate according to Method C1a to afford 2-(2-methyl-4-nitrophenylimino)-5,5-dimethyl-1,3-thiazolidine. The thiazolidine was reacted with 2-methylprop-2-en-1-yl bromide according to Method D2g to afford 2-(2-methyl-4-nitrophenylimino)-3-(2-methylprop-2-en-1-yl)-5,5-dimethyl-1,3-thiazolidine HBr salt.

Sources & evidence

ORD record
ord-9124ed4d6ff44498b6ee3fe41a02e546
Source dataset
uspto-grants-2002_03
Patent number
US06353006B1

Reaction notes

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