1-Bromo-2-methylpropane → HCID 18316099, compound

HRID 276529Notes

Reaction equation

HRID 276529 reaction equation
[Cl:1][C:2]1[C:7]([Cl:8])=[CH:6][CH:5]=[CH:4][C:3]=1[N:9]=[C:10]1[NH:14][CH2:13][C:12]([CH3:16])([CH3:15])[S:11]1.[CH2:17](Br)[CH:18]([CH3:20])[CH3:19]>>[Cl:1][C:2]1[C:7]([Cl:8])=[CH:6][CH:5]=[CH:4][C:3]=1[N:9]=[C:10]1[N:14]([CH2:17][CH:18]([CH3:20])[CH3:19])[CH2:13][C:12]([CH3:16])([CH3:15])[S:11]1

Participants

3

Reactant 2

HCID 65551-Bromo-2-methylpropaneHCID 178428573HCID 178428573, compound

Product 1

HCID 18316099HCID 18316099, compound

Procedure

2-Methyl-2-hydroxypropylamine was reacted with SOCl2 followed by 2,3-dichlorophenyl isothiocyanate according to Method C1a to afford 2-(2,3-dichlorophenylimino)-5,5dimethyl-1,3-thiazolidine. The thiazolidine was reacted with isobutyl bromide according to Method D2g to afford 2-(2,3-dichlorophenylimino)-3-isobutyl-5,5-dimethyl-1,3-thiazolidine.

Sources & evidence

ORD record
ord-12c6de2996fa42f2beaf353e71cb9687
Source dataset
uspto-grants-2002_03
Patent number
US06353006B1

Reaction notes

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