HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pentane, 3-(bromomethyl)- → HCID 18316041, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pentane, 3-(bromomethyl)- | HCID 77432 | — |
| Reactant | 2-(2-Methyl-4-nitrophenylimino)-3-thia-1-azaspiro[4.4]nonane | HCID 178428736 | — |
| Product | HCID 18316041 | HCID 18316041 | — |
Reaction Steps
1-(Hydroxymethyl)cyclopentanamine was prepared according to Method B1c. The 2-hydroxyethylamine was sequentially reacted with SOCl2 and 2-methyl-4-nitrophenyl isothiocyanate according to Method C2a to give 2-(2-methyl-4-nitrophenylimino)-3-thia-1-azaspiro[4.4]nonane. The thiazolidine was reacted with 1-bromo-2-ethylbutane according to Method D2a to afford 2-(2-methyl-4-nitrophenylimino)-1-(2-ethyl-1-butyl)-3-thia-1-azaspiro[4.4]nonane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06353006B1 |
| Source dataset | uspto-grants-2002_03 |
| ORD ID | ord-5a43a599d288412f8edb0ae794d6d1ed |
| Source note | uspto-grants-2002_03 |