Chloroacetic Acid → 2-(2,4,6-Trichlorophenylimino)-3-(2-butyl)-1,3-thiazolidin-4-one

HRID 276683Notes

Reaction equation

[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[C:4]([Cl:9])[C:3]=1[N:10]=[C:11]=[S:12].[CH3:13][CH:14]([NH2:17])[CH2:15][CH3:16].Cl[CH2:19][C:20](O)=[O:21]>>[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[C:4]([Cl:9])[C:3]=1[N:10]=[C:11]1[N:17]([CH:14]([CH2:15][CH3:16])[CH3:13])[C:20](=[O:21])[CH2:19][S:12]1

Participants

Reactant 3

HCID 300Chloroacetic Acid

HCID 24874Sec-Butylamine

HCID 1233992,4,6-Trichlorophenyl isothiocyanate

Product 1

HCID 542310452-(2,4,6-Trichlorophenylimino)-3-(2-butyl)-1,3-thiazolidin-4-one

Procedure

2,4,6-Trichlorophenyl isothiocyanate was reacted with 2-butylamine followed by chloroacetic acid according to Method C8a to afford 2-(2,4,6-trichlorophenylimino)-3-(2-butyl)-1,3-thiazolidin-4-one.

Sources & evidence

ORD record: ord-3234b60a2c4047c6838cef90c4f95db7
Source dataset: uspto-grants-2002_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06353006B1

Reaction notes

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