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HRID2769

反应详情

EQUATION

反应方程式

HRID 2769 的结构方程式

REACTANTS

反应物

2
结构：O=S(=O)(Cl)c1ccc(-c2ccc(Cl)s2)s1
HCID22017280

未命名化合物

结构：Cl.N#Cc1cccc(CN2CC[C@H](N)C2=O)c1
HCID22870786

未命名化合物

PRODUCTS

生成物

1
结构：N#Cc1cccc(CN2CC[C@H](NS(=O)(=O)c3ccc(-c4ccc(Cl)s4)s3)C2=O)c1
HCID86752312

未命名化合物

PROCEDURE

实验过程

The title compound is prepared from 3-(3-(S)-amino-2-oxo-pyrrolidin-1-ylmethyl)-benzonitrile hydrochloride as described in EXAMPLE 1, Part E using 5'-chloro-[2,2']bithiophenyl-5-sulfonyl chloride in place of benzo[b]thiophene-2-sulfonyl chloride. The crude product is triturated with EtOAc/CH2Cl2 to yield a beige solid.

WORKUP

后处理

  1. customThe crude product is triturated with EtOAc/CH2Cl2
  2. customto yield a beige solid