3-Phenylprop-2-enenitrile → 2,7-Diphenyl-[1,2,4]triazolo[1,5-a]pyridin-5-ylamine
Reaction equation
C1(S([CH2:10][C:11]2[N:15]=[C:14]([C:16]3[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=3)[NH:13][N:12]=2)(=O)=O)C=CC=CC=1.[C:22](#[N:31])[CH:23]=[CH:24][C:25]1[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=1>>[C:16]1([C:14]2[N:15]=[C:11]3[CH:10]=[C:24]([C:25]4[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=4)[CH:23]=[C:22]([NH2:31])[N:12]3[N:13]=2)[CH:17]=[CH:18][CH:19]=[CH:20][CH:21]=1Participants
3
Procedure
The title compound, mp. 214-216° C., was prepared in accordance with the general method of example 22 from 3-benzenesulfonylmethyl-5-phenyl-1H-[1,2,4]triazole and cinnamonitrile.
Sources & evidence
- ORD record
- ord-89284d80fe36467c8064146a0b94394a
- Source dataset
- uspto-grants-2002_03
- Patent number
- US06355653B1
Reaction notes
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