HuagongsheHuagongshe Chemistry Print Report · For research reference only
Indole-3-Carboxaldehyde → HCID 135596679, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Indole-3-Carboxaldehyde | HCID 10256 | — |
| Reactant | 4-Bromo-2,6-diaminopyridine | HCID 11435393 | — |
| Reactant | O-(2,4,6-Trimethylbenzenesulfonyl)hydroxylamine | HCID 11830845 | — |
| Product | HCID 135596679 | HCID 135596679 | — |
Reaction Steps
The title compound, MS m/e (%): 328 (M+, 100), was prepared in accordance with the general method of example 63 from 4-bromo-pyridine-2,6-diamine, O-mesitylene-sulfonyl-hydroxylamine, and indole-3-carboxaldehyde. The purification was performed with reversed phase HPLC eluting with an acetonitrile/water gradient.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06355653B1 |
| Source dataset | uspto-grants-2002_03 |
| ORD ID | ord-d2b3718a18f5452aa763e2398dfd6225 |
| Source note | uspto-grants-2002_03 |