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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 277199Generated: October 30, 2026

Hydrochloric Acid → HCID 69692374, compound

https://huagongshe.com/reaction/277199

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 18682354HCID 18682354—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 69692374HCID 69692374—

Reaction Steps

A solution of 3-[3-(1-tert-butoxycarbonylamino-3-methyl-butyl)-isoxazol-5-yl]-3-oxo-propionic acid ethyl ester (1.4 g, 3.9 mmol) in 4M HCl in dioxane (5 ml) was stirred at room temperature. After 3 h the mixture was concentrated under reduced pressure to give the title compound as a pale yellow solid. MS [M+1]+269.0.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06355662B1
Source datasetuspto-grants-2002_03
ORD IDord-3b449bc0b4fc4a8d87db93878082bcf2
Source noteuspto-grants-2002_03