HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 69692374, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 18682354 | HCID 18682354 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 69692374 | HCID 69692374 | — |
Reaction Steps
A solution of 3-[3-(1-tert-butoxycarbonylamino-3-methyl-butyl)-isoxazol-5-yl]-3-oxo-propionic acid ethyl ester (1.4 g, 3.9 mmol) in 4M HCl in dioxane (5 ml) was stirred at room temperature. After 3 h the mixture was concentrated under reduced pressure to give the title compound as a pale yellow solid. MS [M+1]+269.0.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06355662B1 |
| Source dataset | uspto-grants-2002_03 |
| ORD ID | ord-3b449bc0b4fc4a8d87db93878082bcf2 |
| Source note | uspto-grants-2002_03 |