HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 54153740, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 54051298 | HCID 54051298 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 54153740 | HCID 54153740 | — |
Reaction Steps
A solution of 2-[5-(2-Methoxycarbonyl-ethyl)-thiazol-2-yl]-pyrrolidine-1-carboxylic acid tert-butyl ester (0.37 g, 1.09 mmol) in a solution of hydrochloric acid in dioxane (4N, 10 mL) was stirred at room temperature for 1 h. The solvent was removed in vacuo and the residue dissolved in methylene chloride. The methylene chloride was removed in vacuo and the residue dissolved again in methylene chloride. The solvent was removed in vacuo and the residue used without purification. MS: Calc'd for C11H16N2O2S: 240.09. Found (M+1): 241.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06355662B1 |
| Source dataset | uspto-grants-2002_03 |
| ORD ID | ord-5954cc9d052941429e864fc05e7d26e5 |
| Source note | uspto-grants-2002_03 |