HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 1-methyl-1H,4H,5H,6H,7H-imidazo[4,5-c]pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 178420865 | HCID 178420865 | — |
| Product | 1-methyl-1H,4H,5H,6H,7H-imidazo[4,5-c]pyridine | HCID 929096 | — |
Reaction Steps
Operating as in Example 1, but starting from 4,5,6,7-tetrahydroimidazo-[4,5-c]-pyridine and methyl iodide, 1-Methyl-4,5,6,7-tetrahydroimidazo-[4,5-c]-pyridine is obtained as intermediate and successively reacted with methyl isothiocyanate to give 1-Methyl-5-(N-methylthiocarbamoyl)-4,5,6,7-tetrahydroimidazo-[4,5-c]-pyridine in a 78% yield, m.p. 238° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04223146 |
| Source dataset | uspto-grants-1980_09 |
| ORD ID | ord-f69abc026200451db69fe26f9ec86191 |
| Source note | uspto-grants-1980_09 |