HRID277561

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CC1(C)CCC(=O)c2ccc(C#Cc3ccc(C(=O)O)cc3)cc21

HCID15345547

未命名化合物

2 次

结构：CC1(C)CC=C(C#N)c2cc(C#Cc3ccc(C(=O)O)cc3)ccc21

HCID23001771

未命名化合物

PRODUCTS

生成物

结构：CC1(C)CC=C(C#N)c2ccc(C#Cc3ccc(C(=O)O)cc3)cc21

HCID18314578

未命名化合物

PROCEDURE

实验过程

Employing the same general procedure as for the preparation of 4-[(8-cyano-7,8-dihydro-8,8-dimethylnaphth-3-yl)ethynyl]benzoic acid (Compound 129), 63 mg (0.26 mmol) of 4-[(5,6,7,8-tetrahydro-8,8-dimethyl-5-oxonaphth-2-yl)ethynyl]benzoic acid (Compound 7) was converted into the title compound (yellow powder) using 0.06 ml (0.54 mmol) of cyanotrimethylsilane and 6 drops of boron trifluoride etherate.