HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Triethylamine → HCID 22625351, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Triethylamine | HCID 8471 | — |
| Edukt | ((p-(Benzyloxy)phenoxy)methyl)oxirane | HCID 119882 | — |
| Edukt | HCID 22625378 | HCID 22625378 | — |
| Lösungsmittel | 1,4-Dioxane | HCID 31275 | — |
| Produkt | HCID 22625351 | HCID 22625351 | 67,3% |
Reaktionsschritte
Using 1.56 g of 1-(4-benzyloxyphenoxy)-2,3-epoxypropane, 1.80 g of 1-(2,4-dimethoxyphenyl)piperazine dihydrochloride, 1.9 ml of triethylamine and 50 ml of dioxane, reaction and workup were carried out as in Example 1-A. Purification by column chromatography (silica gel, elution with ethyl acetate:hexane =1:0.5) gave 1.96 g of pale red crystals, m.p. 110-112° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06358515B2 |
| Quelldatensatz | uspto-grants-2002_03 |
| ORD ID | ord-0f1cbbe117464338a1abcdc98b305f2c |
| Quellennotiz | uspto-grants-2002_03 |