Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3H-Indole, 2,3,3-trimethyl- → n-(5-Carboxypentyl)-2,3,3-trimethylindolinium bromide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3H-Indole, 2,3,3-trimethyl- | HCID 15427 | — |
| 반응물 | 6-Bromohexanoic acid | HCID 20210 | — |
| 생성물 | n-(5-Carboxypentyl)-2,3,3-trimethylindolinium bromide | HCID 18764706 | — |
반응 단계
N-(5-carboxypentyl)-2,3,3-trimethylindolinium bromide was prepared by the process set forth in Example IA with 2,3,3-trimethylindolenine and 6-bromohexanoic acid to produce 2.43 grams (71.2 percent yield) of yellow crystals. 1H and 13C NMR spectra indicated the following:
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06358655B1 |
| 출처 데이터셋 | uspto-grants-2002_03 |
| ORD ID | ord-3899277ff86e4ff982f05beaa57e671e |
| 출처 메모 | uspto-grants-2002_03 |