Acetone → HCID 9861056, compound

HRID 277840Notes

Reaction equation

HRID 277840 reaction equation
[NH2:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[CH:13]=[CH:12][CH:11]=[C:10]([N+:14]([O-:16])=[O:15])[CH:9]=2)=[CH:4][C:3]=1[CH:17]([OH:19])[CH3:18].[CH3:20][C:21]([CH3:23])=O>O>[N+:14]([C:10]1[CH:9]=[C:8]([C:5]2[CH:6]=[CH:7][C:2]3[NH:1][C:21]([CH3:23])([CH3:20])[O:19][CH:17]([CH3:18])[C:3]=3[CH:4]=2)[CH:13]=[CH:12][CH:11]=1)([O-:16])=[O:15]

Participants

4

Reactant 2

HCID 180AcetoneHCID 23435599HCID 23435599, compound

Product 1

HCID 9861056HCID 9861056, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Prepared from 1-(4-amino-3′-nitro-biphenyl-3-yl)-ethanol and acetone in the same fashion as that of Example 4. Yellow solid: mp 188-189° C.; Anal. Calc. For C17H18N2O3.0.35 H2O: C, 67.02; H, 6.19; N, 9.20. Found: C, 66.7; H, 5.89; N, 9.03.

Sources & evidence

ORD record
ord-2eb67751f29f4860be57999e1d09bd11
Source dataset
uspto-grants-2002_03
Patent number
US06358948B1

Reaction notes

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