HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminium lithium hydride → 2-(3-Methoxy-phenyl)-4-methyl-pentylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | HCID 22626833 | HCID 22626833 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 2-(3-Methoxy-phenyl)-4-methyl-pentylamine | HCID 22626844 | 93.8% |
Reaction Steps
By working in a way similar to that described in example 17 but using LiAlH4 (0.7 g, 0.018 moles) in anhydrous ethyl ether (35 ml) and 2-(3-methoxy-phenyl)-4-methyl-pentan-nitrile (3.8 g, 0.018 moles), obtained as described in example 20, in anhydrous ethyl ether (35 ml), 3.5 g of the title compound were obtained (yield: 90.4%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06358973B1 |
| Source dataset | uspto-grants-2002_03 |
| ORD ID | ord-151e1751a9144f2e8d81db96c30b2620 |
| Source note | uspto-grants-2002_03 |