1,1'-Carbonyldiimidazole → HCID 22626841, compound

Participants

Reaction Steps

By working in a way similar to that described in example 30 but using (3,5-dichloro-pyridin-4-yl)-acetic acid (4.62 g, 22.4 mmoles), carbonyldiimidazole (4 g, 24.64 mmoles), THF (60 ml) and 2-(3-methoxy-phenyl)-3-methyl-butylamine (4.33 g, 22.4 mmoles), obtained as described in example 37, 8.36 g of the title compound were obtained (yield: 97.9%), m.p.: 94-95° C.

Provenance & Evidence