5-Chloroindole → HCID 9903606, compound

Participants

Reaction Steps

5-Chloro-1H-indole (1.00 g, 6.63 mmol) and 7-octahydroindolizinone (1.39 g, 9.95 mmol) were converted to product by the procedure of Preparation 17 to give 595 mg. (33.1%). EA calculated for C16H17N2Cl: C, 70.45; H, 6.28; N, 10.27. Found: C, 70.60; H, 6.46; N, 10.28. MS(FD) (m/e): 272.

Provenance & Evidence