HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Amino-3-nitrobenzoic acid → 2,3-Diaminobenzoic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Amino-3-nitrobenzoic acid | HCID 219633 | — |
| Edukt | HCID 178418361 | HCID 178418361 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | 2,3-Diaminobenzoic acid | HCID 198069 | — |
Reaktionsschritte
14 g (76.9 mmol) of 2-amino-3-nitrobenzoic acid (1b) were dissolved in 500 ml of methanol, treated with Pd/C, and hydrogenated with hydrogen. After 4 h, the catalyst was filtered off with suction and concentrated. A dark-brown solid was obtained. Yield: 11.67 g (99%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06358978B1 |
| Quelldatensatz | uspto-grants-2002_03 |
| ORD ID | ord-2b175d8949474a819a64b0b78c04ef77 |
| Quellennotiz | uspto-grants-2002_03 |