HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Azido-3-(3-methoxyphenyl)-1-phenylpropane → 3-(3-Methoxyphenyl)-1-phenylpropylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Azido-3-(3-methoxyphenyl)-1-phenylpropane | HCID 22627107 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 3-(3-Methoxyphenyl)-1-phenylpropylamine | HCID 22627103 | — |
Reaction Steps
A solution of the product from Step B (1.08 g, 3.7 mmol) in 30 mL of EtOH containing Pd/C (10%, 100 mg) was stirred at ambient temperature under 1 Atm. of H2 for 20 hours. The reaction mixture was filtered to provide the title product as a clear colorless oil which was sufficiently pure for use in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06358985B1 |
| Source dataset | uspto-grants-2002_03 |
| ORD ID | ord-9d0a4ee5be92430b8bf18e32271c5dab |
| Source note | uspto-grants-2002_03 |