HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 131723146, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 18187525 | HCID 18187525 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 131723146 | HCID 131723146 | — |
Reaction Steps
To a solution of 1-(t-butoxycarbonyl)-4-(3-(2-pyridyl)propyl)piperidine (from Step A) (128 mg, 0.42 mmol) in methylene chloride (1 mL) was added TFA (1 mL). After stirring for 2 h at rt, the reaction was concentrated to give the title compound (36 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06358979B1 |
| Source dataset | uspto-grants-2002_03 |
| ORD ID | ord-778ca910838e488a87ddfbe3b9ccdb04 |
| Source note | uspto-grants-2002_03 |