HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethanolamine → HCID 11107026, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethanolamine | HCID 8113 | — |
| Reactant | 4-Methyloxybenzyl chloride | HCID 69993 | — |
| Product | HCID 11107026 | HCID 11107026 | — |
Reaction Steps
2-[(2-Hydroxy-ethyl)-(4-methoxy-benzyl)-amino]-ethanol was prepared according to the general method as outlined in Example 1 (Step 4). Starting from diethanolamine (10.5 g, 100 mmol). and 4-methoxy benzyl chloride (15.6 g, 100 mmol). Yield 21 g, (98%); yellow oil; MS: 226 (M+H)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06358980B1 |
| Source dataset | uspto-grants-2002_03 |
| ORD ID | ord-69e42038a45c428085e0c347335bbc19 |
| Source note | uspto-grants-2002_03 |