HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethanolamine → HCID 11042091, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethanolamine | HCID 8113 | — |
| Reactant | 4-Fluorobenzyl chloride | HCID 9602 | — |
| Product | HCID 11042091 | HCID 11042091 | — |
Reaction Steps
2-[(4-Fluoro-benzyl)-(2-hydroxy-ethyl)-amino]-ethanol was prepared according to the general method as outlined in Example 1 (Step 4). Starting from diethanolamine (15.7 g, 150 mmol), and 4-fluoro-benzyl chloride (14.4 g, 100 mmol) 20 g of the product was isolated. Yield 20 g, (93%%); yellow oil; MS: 215 M+H)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06358980B1 |
| Source dataset | uspto-grants-2002_03 |
| ORD ID | ord-d00ab2d0c8ab4e4eb47fdaaad5400aba |
| Source note | uspto-grants-2002_03 |