HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-2-butyne → Ethyl{[3-(2-butynyloxy)phenyl]sulfanyl}acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-2-butyne | HCID 2756862 | — |
| Reactant | Ethyl [(3-hydroxyphenyl)sulfanyl]acetate | HCID 57418561 | — |
| Product | Ethyl{[3-(2-butynyloxy)phenyl]sulfanyl}acetate | HCID 23513827 | 100% |
Reaction Steps
Ethyl{[3-(2-butynyloxy)phenyl]sulfanyl}acetate was prepared according to the general method as outlined in example 1 (step 2), starting from ethyl [(3-hydroxyphenyl)sulfanyl]acetate (3.87 g, 18.3 mmol) and 4-bromo-2-butyne (2.66 g, 20 mmol); 5.16 g yellow oil. Yield 100%; MS(EI): 264.1 (M+H)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06358980B1 |
| Source dataset | uspto-grants-2002_03 |
| ORD ID | ord-3d5d5127792c49ed9c4d9874c8148a5a |
| Source note | uspto-grants-2002_03 |