HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pivalic acid → n-Neopentanoyl-2-butyloctylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pivalic acid | HCID 6417 | — |
| Reactant | 2-Butyl-n-octan-1-amine | HCID 18673284 | — |
| Solvent | Heptane | HCID 8900 | — |
| Product | n-Neopentanoyl-2-butyloctylamine | HCID 18673286 | 76% |
Reaction Steps
10.4 g of pivalic acid and 17.2 g of 2-butyloctylamine were mixed together in the tube of a microwave machine (Maxidigest™ MX 350 from the company Prolabo; frequency 2450±50 MHz, modulable power 300 W). After irradiation for about 1 hour at 160° C.±10° C., the reaction mixture was dissolved in heptane and then purified on silica. 19 g of the desired amide were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06359175B1 |
| Source dataset | uspto-grants-2002_03 |
| ORD ID | ord-8b27d062e00d4dcfacb35b68adc53cff |
| Source note | uspto-grants-2002_03 |