HuagongsheHuagongshe Chemistry Print Report · For research reference only
9-(4-Methoxy-2,6-dimethyl-phenyl)-3,7-dimethyl-nona-2,4,6,8-tetraen-1-oic acid butyl ester → 9-(4-Methoxy-2,6-dimethyl-phenyl)-3,7-dimethyl-nona-2,4,6,8-tetraen-1-oic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 9-(4-Methoxy-2,6-dimethyl-phenyl)-3,7-dimethyl-nona-2,4,6,8-tetraen-1-oic acid butyl ester | HCID 53661015 | — |
| Reactant | Butyl 3,7-dimethyl-8-oxoocta-2,4,6-trienoate | HCID 53845956 | — |
| Reactant | 4-Methoxy-2,6-dimethyl-benzyl-triphenylphosphonium chloride | HCID 86735899 | — |
| Product | 9-(4-Methoxy-2,6-dimethyl-phenyl)-3,7-dimethyl-nona-2,4,6,8-tetraen-1-oic acid | HCID 53899576 | — |
Reaction Steps
By the procedure described in Example 14, 9-(4-methoxy-2,6-dimethyl-phenyl)-3,7-dimethyl-nona-2,4,6,8-tetraen-1-oic acid butyl ester is manufactured from 4-methoxy-2,6-dimethylbenzyl-triphenylphosphonium chloride by reaction with 7-formyl-3-methyl-octa-2,4,6-trien-1-oic acid butyl ester. From this product, there is produced by the procedure of Example 15, 9-(4-methoxy-2,6-dimethyl-phenyl)-3,7-dimethyl-nona-2,4,6,8-tetraen-1-oic acid of melting point 207°-208° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04224244 |
| Source dataset | uspto-grants-1980_09 |
| ORD ID | ord-e562e256eefb44969f1c634265522511 |
| Source note | uspto-grants-1980_09 |