HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-[3-(5-Cyano-1-ethyl-1,6-dihydro-4-methyl-2,6-dioxo-3(2H)-pyridinylidene)-1-propen-1-yl]-1-ethyl-1,2-dihydro-6-hydroxy-4-methyl-2-oxo-3-pyridinecarbonitrile → HCID 86757896, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-[3-(5-Cyano-1-ethyl-1,6-dihydro-4-methyl-2,6-dioxo-3(2H)-pyridinylidene)-1-propen-1-yl]-1-ethyl-1,2-dihydro-6-hydroxy-4-methyl-2-oxo-3-pyridinecarbonitrile | HCID 119884 | — |
| Reactant | Ammonium Acetate | HCID 517165 | — |
| Reactant | Triethylammonium | HCID 1385867 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 86757896 | HCID 86757896 | — |
Reaction Steps
4.9 g of commercial triethylammonium 5-(3-(5-cyano-1-ethyl-4-methyl-2,6-dioxo-1,6-dihydro-2H -pyridin-3-ylidene)propenyl-1-ethyl-6-hydroxy-4-methyl-2-oxo-1,2-dihydropyridine-3-carbonitrile (24a) was made to react with 0.8 g of ammonium acetate in 75 mL of acetic acid as described under (a). This gave 3.6 g of dye (24a).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06361571B1 |
| Source dataset | uspto-grants-2002_03 |
| ORD ID | ord-b7d91f0df61f4c0e8bf75f4751a6edba |
| Source note | uspto-grants-2002_03 |