HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 3-(2-Hydroxyethylhydrazino)-6-(3,5-dimethyl-1-pyrazolyl)-pyridazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 2-Hydrazinoethanol | HCID 8017 | — |
| Reactant | 3-Chloro-6-(3,5-dimethylpyrazol-1-yl)pyridazine | HCID 321073 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 3-(2-Hydroxyethylhydrazino)-6-(3,5-dimethyl-1-pyrazolyl)-pyridazine | HCID 54036303 | — |
Reaction Steps
A mixture of 2.09 g (0.01 moles) of 3-chloro-6-(3,5-dimethyl-1-pyrazolyl)-pyridazine, 30 ml of ethanol and 1.52 g (0.02 moles) of hydroxyethyl hydrazine is reacted and worked up in the same way as described in Example 42. Yield: 0.3 g (10.5%); the hydrochloride melts at 302°-305° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04224325 |
| Source dataset | uspto-grants-1980_09 |
| ORD ID | ord-92350680f6dd4a6e8f7418eba77a39b7 |
| Source note | uspto-grants-1980_09 |