HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 22623932, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | HCID 22624013 | HCID 22624013 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 22623932 | HCID 22623932 | — |
Reaction Steps
Following the procedure of Example W1, a mixture of the 2-allyloxy-5-bromo-7-nitro-benzo[de] isoquinoline-1,3-dione from above, pyrrolidine (0.43 g, 6.0 mmol) and triethyl amine (1.2 g, 12 mmol) in DMF (10 mL) was reacted to give 0.91 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06362181B1 |
| Source dataset | uspto-grants-2002_03 |
| ORD ID | ord-b94e6ca8b4b14912b5c157e6304ca53a |
| Source note | uspto-grants-2002_03 |