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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 278973Generated: October 30, 2026

Triethylamine → HCID 22623960, compound

https://huagongshe.com/reaction/278973

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTriethylamineHCID 8471—
ReactantPyrrolidineHCID 31268—
ReactantHCID 22624031HCID 22624031—
SolventDimethylformamideHCID 6228—
ProductHCID 22623960HCID 2262396096.2%

Reaction Steps

Following the procedure of Example W1, 2-allyloxy-5-methyl-7-nitro-benzo[de]isoquinoline-1,3-dione (0.52 g, 1.7 mmol, from Example 12), pyrrolidine (0.23 g, 3.2 mmol), triethyl amine (0.65 g, 6.4 mmol) in DMF (5 mL) were reacted to give 0.55 g of the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06362181B1
Source datasetuspto-grants-2002_03
ORD IDord-9e964c47824b4ff985330c2027301681
Source noteuspto-grants-2002_03