HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 22623960, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | HCID 22624031 | HCID 22624031 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 22623960 | HCID 22623960 | 96.2% |
Reaction Steps
Following the procedure of Example W1, 2-allyloxy-5-methyl-7-nitro-benzo[de]isoquinoline-1,3-dione (0.52 g, 1.7 mmol, from Example 12), pyrrolidine (0.23 g, 3.2 mmol), triethyl amine (0.65 g, 6.4 mmol) in DMF (5 mL) were reacted to give 0.55 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06362181B1 |
| Source dataset | uspto-grants-2002_03 |
| ORD ID | ord-9e964c47824b4ff985330c2027301681 |
| Source note | uspto-grants-2002_03 |