HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22623948, compound → HCID 22624022, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22623948 | HCID 22623948 | — |
| Reactant | HCID 178525683 | HCID 178525683 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 22624022 | HCID 22624022 | 91.8% |
Reaction Steps
Following the procedure of Example 52, 2-benzyloxy-5-bromo-6-dimethylamino-benzo[de]isoquinoline-1,3-dione (0.17 g, 0.39 mmol, from Example X1) and a 1.0 M solution of boron tris(trifluoroacetate) in TFA (2 mL) were reacted to give 0.12 g of the title compound, mp 185-187° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06362181B1 |
| Source dataset | uspto-grants-2002_03 |
| ORD ID | ord-21409e203bff4c7da9cf447298d048dd |
| Source note | uspto-grants-2002_03 |